反应条件
in toluene (N2); using Schlenk techniques; addn. of soln. of Au(C6H3(CH2NMe2)2)(PPh3) (1 equiv.) in toluene to soln. of anhyd. FeCl3 (1 equiv.) in degassed, dry toluene; stirring for 5 h at room temp.; removal of solvent in vac., extn. with degassed, dry Et2O, pptn., transferring of soln. to another flask by cannula, concn., cooling at -20°C, crystn.;
参考文献
Contel, Maria; Stol, Marianne; Casado, Miguel A.; Van Klink, Gerard P.M.; Ellis, Dianne D.; Spek, Anthony L.; Van Koten, Gerard
Organometallics, 2002 , vol. 21, # 21 p. 4556 - 4559
