2-丙-2-烯基硫基苯胺合成路线 (共 11 条)
反应条件
sodium hydroxide in benzene 48 h; Heating;
参考文献
Shadakshari; Talukdar; Chattopadhyay
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 1007 - 1010
反应条件
titanium(III) chloride; lithium in tetrahydrofuran T=25°C; 2 h;
参考文献
Shadakshari; Talukdar; Chattopadhyay
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 1007 - 1010
反应条件
1: 47 percent / TiCl3; Li / tetrahydrofuran / 2 h / 25 °C 2: 45 percent / K2CO3 / ethanol / 0 °C View Scheme
参考文献
Shadakshari; Talukdar; Chattopadhyay
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 1007 - 1010
反应条件
1: 47 percent / TiCl3; Li / tetrahydrofuran / 2 h / 25 °C 2: 48 percent / K2CO3 / ethanol / 0 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 40, # 10 p. 1007 - 1010
反应条件
sodium hydroxide in methanol
2 h; Ambient temperature;
参考文献
Uchida; Otsubo; Matsubara; Ohtani; Morita; Yamasaki
Chemical and Pharmaceutical Bulletin, 1995 , vol. 43, # 4 p. 693 - 698
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=90°C; 8 h; Inert atmosphere; chemoselective reaction;
参考文献
Saha, Amit; Ranu, Brindaban C.
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1902 - 1905
反应条件
potassium carbonate in ethanol
T=0°C;
参考文献
Shadakshari; Talukdar; Chattopadhyay
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 1007 - 1010
反应条件
1: 55 percent / TiCl3; Li / tetrahydrofuran / 20 h / Heating
2: 58 percent / K2CO3 / ethanol / 0 °C
View Scheme
参考文献
Shadakshari; Talukdar; Chattopadhyay
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 1007 - 1010
反应条件
hydrogenchloride; iron; copper dichloride
参考文献
Brand
Archiv der Pharmazie (Weinheim, Germany), 1935 , vol. 273, p. 65,75,76
反应条件
1: 47 percent / TiCl3; Li / tetrahydrofuran / 2 h / 25 °C
2: 68 percent / K2CO3 / ethanol / 0 °C
View Scheme
参考文献
Shadakshari; Talukdar; Chattopadhyay
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2001 , vol. 40, # 10 p. 1007 - 1010