2,3,4,5,6-五氟甲苯合成路线 (共 52 条)
反应条件
1: Cl2 / Irradiation 2: aq. K2CO3 / Heating View Scheme
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
bromine in tetrachloromethane
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
N-bromosuccinmide T=36°C; 18 h; Irradiationneat (no solvent);
参考文献
Jereb, Marjan; Zupan, Marko; Stavber, Stojan
Helvetica Chimica Acta, 2009 , vol. 92, # 3 p. 555 - 566
反应条件
1: methanol 2: Br2 / CCl4 3: (i) NaOEt, EtOH, (ii) /BRN= 2529288/, DMF 4: aq. HI View Scheme
参考文献
Filler,R. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 3 p. 534 - 538
反应条件
1: Br2 / Irradiation 2: (i) Mg, I2, (ii) /BRN= 1900390/ View Scheme
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
sulfuryl dichloride; dibenzoyl peroxide
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
1: N2H4*H2O / dioxane / Heating 2: aq. CuSO4 3: (i) nBuLi, (ii) /BRN= 1900390/, (iii) aq. HCl View Scheme
参考文献
Tamborski,C.; Soloski,E.J.
Journal of Organic Chemistry, 1966 , vol. 31, p. 746 - 749
反应条件
1: Cl2 / Irradiation 2: aq. ethanol 3: aq. H2SO4, AcOH 4: FSO3H 5: LiAlH4 View Scheme
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
1: Cl2 / Irradiation 2: aq. ethanol View Scheme
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
1: N2H4*H2O / dioxane / Heating 2: aq. CuSO4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 31, p. 746 - 749