2,3,4,5,6-五氟甲苯合成路线 (共 52 条)
反应条件
1: Br2 / CCl4 2: (i) NaOEt, EtOH, (ii) /BRN= 647808/, DMF 3: aq. HCl View Scheme
参考文献
Filler,R. et al.
Journal of Organic Chemistry, 1969 , vol. 34, # 3 p. 534 - 538
反应条件
in methanol 136 h; Heating;
参考文献
Filler, Robert; Rickert, Robert C.
Journal of Fluorine Chemistry, 1981 , vol. 18, p. 483 - 496
参考文献
Shtark, A. A.; Chuikova, T. V.; Shteingarts, V. D.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 5 p. 960 - 967
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 5 p. 1055 - 1063
反应条件
1: Br2 / Irradiation
2: 180 - 200 °C
View Scheme
参考文献
Birchall,J.M.; Haszeldine,R.N.
Journal of the Chemical Society, 1961 , p. 3719 - 3727
反应条件
chlorine
Irradiation;
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
chlorine
Irradiation;
参考文献
Birchall,J.M.; Haszeldine,R.N.
Journal of the Chemical Society, 1961 , p. 3719 - 3727
反应条件
1: Cl2 / Irradiation
2: aq. ethanol
3: H2SO4
View Scheme
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
1: Br2 / Irradiation
2: Mg, I2
View Scheme
参考文献
Birchall,J.M.; Haszeldine,R.N.
Journal of the Chemical Society, 1961 , p. 3719 - 3727
反应条件
N-bromosuccinmide
T=36°C; 18 h; Irradiationneat (no solvent);
参考文献
Jereb, Marjan; Zupan, Marko; Stavber, Stojan
Helvetica Chimica Acta, 2009 , vol. 92, # 3 p. 555 - 566
反应条件
hydrazine hydrate in 1,4-dioxane
Heating;
参考文献
Tamborski,C.; Soloski,E.J.
Journal of Organic Chemistry, 1966 , vol. 31, p. 746 - 749