2,3,4,5,6-五氟苯胺合成路线 (共 126 条)
反应条件
potassium tert-butylate in tetrahydrofuran
T=20°C; 0.0333333 h;
参考文献
Roberts, Kenneth M.; Jones, Jeffery P.
Chemistry - A European Journal, 2010 , vol. 16, # 27 p. 8096 - 8107
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
potassium tert-butylate in tetrahydrofuran
T=20°C; 0.166667 h;
参考文献
Roberts, Kenneth M.; Jones, Jeffery P.
Chemistry - A European Journal, 2010 , vol. 16, # 27 p. 8096 - 8107
反应条件
HCOOH, formaline
18 h in reflux with 90percent HCOOH, at heating for only 6 h an unknown byproduct formed;
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
N,N-dimethyl-aniline in benzene
6 h; Heating;
参考文献
Petrova; Platonov
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 2 p. 218 - 226
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide
T=115°C; P=4912.9 Torr; 22 h;
参考文献
Perry, Robert J.; Wilson, B. David
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6351 - 6354
反应条件
in benzene
T=20°C; 96 h;
参考文献
Petrova; Platonov
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 2 p. 218 - 226
反应条件
1: NaOCl
3: NaOMe / methanol
4: aq. H2O2, (CF3CO)2O
View Scheme
参考文献
Burdon,J. et al.
Journal of the Chemical Society, 1965 , p. 2621 - 2627
反应条件
1: aq. H2O2, (CF3CO)2O / CH2Cl2 / Heating
2: NH3 / diethyl ether / Ambient temperature
View Scheme
参考文献
Brooke,G.M. et al.
Journal of the Chemical Society, 1961 , p. 802 - 807