2,3,4,5,6-五氟苯胺合成路线 (共 126 条)
反应条件
2,3,4,5,6-pentafluorobenzaldehyde in ethanol T=70°C; 5 h;
参考文献
Journal of Fluorine Chemistry, , vol. 36, p. 247 - 272
反应条件
ammonium chloride; zinc in water T=50°C;
参考文献
Journal of Fluorine Chemistry, , vol. 36, p. 247 - 272
反应条件
bromine in ethanol with ethanolic Br2 soln. at -60°C (2 h);
参考文献
Journal of the Chemical Society, , p. 4966 - 4976
反应条件
ammonia in water T=180°C; 6 h; Autoclave;
参考文献
Russian Chemical Bulletin, , vol. 58, # 4 p. 823 - 827
反应条件
ammonia in water T=180°C; 24 h; Autoclave;
参考文献
Russian Chemical Bulletin, , vol. 58, # 4 p. 823 - 827
反应条件
in diethyl ether T=0 - 20°C; 72 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 50, # 1 p. 29 - 34
Zh. Org. Khim., , vol. 50, # 1 p. 37 - 42,6
反应条件
aluminium trichloride T=60 - 70°C; 17 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, # 6 p. 1168 - 1176
Zhurnal Organicheskoi Khimii, , vol. 22, # 6 p. 1297 - 1306
反应条件
1: morpholine; 4-chloro-2,3,4,5,6-pentafluorocyclohexa-2,5-dienone in diethyl ether 0.5 h; 2: aluminum trichloride-pentafluorophenylhydrazine complex in diethyl ether T=0 - 20°C; 20 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 50, # 1 p. 29 - 34
Zh. Org. Khim., , vol. 50, # 1 p. 37 - 42,6
反应条件
potassium carbonate in water 10 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 11 p. 3447 - 3452
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1562 - 1565