2,3,4,5,6-五氟苯胺合成路线 (共 126 条)
反应条件
ammonia; sodium amide T=-70°C; unter Druck;
参考文献
Chemistry and Industry (London, United Kingdom), , p. 630
Journal of the Chemical Society, , p. 1768,1770
反应条件
aluminium trichloride T=130°C; 9 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 41, # 2 p. 218 - 226
参考文献
Tetrahedron Letters, , vol. 30, # 1717 p. 2199 - 2202
反应条件
acetic acid in water T=25°C; Irradiation; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 62, # 16 p. 5363 - 5370
反应条件
aluminium trichloride T=130°C; 9 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Russian Journal of Organic Chemistry, , vol. 41, # 2 p. 218 - 226
反应条件
aluminium trichloride T=170°C; 17 h; Further byproducts given;
参考文献
Russian Journal of Organic Chemistry, , vol. 41, # 2 p. 218 - 226
反应条件
in diethyl ether T=0 - 20°C; 20 h; Reagent/catalystTimeConcentration; Overall yield = 0.25 g;
参考文献
Russian Journal of Organic Chemistry, , vol. 50, # 1 p. 29 - 34
Zh. Org. Khim., , vol. 50, # 1 p. 37 - 42,6
反应条件
T=-78°C; 4 h; Irradiationfurther temperatures; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 8307 - 8309
反应条件
1: diethyl ether / 0 °C 2: diethyl ether / 72 h / 0 - 20 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 50, # 1 p. 29 - 34
Zh. Org. Khim., , vol. 50, # 1 p. 37 - 42,6
反应条件
in toluene Ambient temperatureIrradiationother solvents and sensitizer; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 113, # 8 p. 3209 - 3211