2,3,4,5,6-五氟苯胺合成路线 (共 126 条)
参考文献
Castellano,J.A. et al.
Journal of Organic Chemistry, 1966 , vol. 31, p. 821 - 824
反应条件
formic acid; dihydrogen peroxide in dichloromethane Heating;
参考文献
Ang, H. G.; Kwik, W. L.; Ong, K. K.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 3 p. 321 - 330
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide T=160°C; P=4912.9 Torr; 3.5 h;
参考文献
Perry, Robert J.; Wilson, B. David
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6351 - 6354
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl acetamide T=160°C; P=4912.9 Torr; 2 h;
参考文献
Perry, Robert J.; Wilson, B. David
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6351 - 6354
反应条件
1: With trifluoroacetic acid; sodium nitrite T=0°C; 1 h; Inert atmosphereSchlenk technique; 2: With sodium azide T=0°C; 1 h; Inert atmosphereSchlenk technique;
参考文献
Jin, Li-Mei; Xu, Xue; Lu, Hongjian; Cui, Xin; Wojtas, Lukasz; Zhang, X. Peter
Angewandte Chemie - International Edition, 2013 , vol. 52, # 20 p. 5309 - 5313
Angew. Chem., 2013 , vol. 125, # 20 p. 5417 - 5421,5
反应条件
iodic acid in ethanol; water T=20°C; 2 h;
参考文献
Bukhtoyarova; Ektova; Alekseev; Beregovaya
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 9 p. 1309 - 1315
反应条件
hydrazine hydrate in 1,4-dioxane Heating;
参考文献
Holland,D.G. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1562 - 1565
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
T=160°C; Substitution; 15 h;
参考文献
Frolov
Russian Journal of Organic Chemistry, 1998 , vol. 34, # 7 p. 1047 - 1051
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84