2,3,4,5,6-五氟苯胺合成路线 （共 126 条）
参考文献
Holland,D.G. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1562 - 1565
反应条件
2: copper bronze View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
1: 81 percent / nitrosonium tetrafluoroborate / acetonitrile / 1 h / -30 °C 2: 44 percent / potassium iodide / acetonitrile / 0.17 h View Scheme
参考文献
Kosynkin, Dmitry; Bockman, T. Michael; Kochi, Jay K.
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 10 p. 2003 - 2012
反应条件
n-Pentyl nitrite T=80°C; 0.5 h; reaction with different substituted benzenes to different products; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 64, # 3 p. 201 - 216
反应条件
copper(I) bromide; sulfuric acid; copper(II) sulfate; potassium bromide; sodium nitrite; B(3,5-bis(trifluoromethyl)phenyl)4- 1) 0 deg C, dichloromethane, water 2) dichloromethane, water, 100 min, rt.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Iwamoto, Hidetoshi; Sonoda, Takaaki; Kobayashi, Hiroshi
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 535 - 537
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
反应条件
in dimethyl sulfoxide Equilibrium constant;
参考文献
Vlasov, V. M.; Terekhova, M. I.; Petrov, E. S.; Shatenshtein, A. I.; Yakobson, G. G.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 10 p. 1807 - 1813
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2025 - 2031
反应条件
Cu2Cl2; sulfuric acid; copper(II) sulfate; sodium nitrite; benzene; B(3,5-bis(trifluoromethyl)phenyl)4- 1) 0 deg C, dichloromethane, water, 2) dichloromethane, water , 100 min, rt.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Iwamoto, Hidetoshi; Sonoda, Takaaki; Kobayashi, Hiroshi
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 535 - 537
反应条件
Cu2Cl2; sulfuric acid; copper(II) sulfate; sodium nitrite; B(3,5-bis(trifluoromethyl)phenyl)4- 1) 0 deg C, dichloromethane, water, 5 min 2) dichloromethane, water 100 min, rt.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Iwamoto, Hidetoshi; Sonoda, Takaaki; Kobayashi, Hiroshi
Journal of Fluorine Chemistry, 1984 , vol. 24, p. 535 - 537
反应条件
2: hydrogenchloride View Scheme
参考文献
Gmelin Handbook: F: PerFHalOrg.7, 1, page 1 - 84
