3-N-苯二甲酰甘氨酸氨基甲基苯胺合成路线 （共 4 条）
反应条件
1: With SnCl2·2H2O in ethanol 6 h; Reflux; 2: With water; sodium hydroxide in ethyl acetate 0.5 h; Cooling with ice;
参考文献
Greff, Zoltán; Varga, Zoltán; Kéri, György; Németh, Gábor; Örfi, László; Szántai Kis, Csaba
Patent: US2012/258968 A1, 2012 ;
Location in patent: Page/Page column 19 ;
反应条件
1.1: N,N-dimethyl-formamide / 20 °C 2.1: SnCl2·2H2O / ethanol / 6 h / Reflux 2.2: 0.5 h / Cooling with ice View Scheme
参考文献
WO2011/77171 A1, ;
WO 2011/077171 A1
反应条件
sulfuric acid T=50°C; 3 h; Title compound not separated from byproducts;
参考文献
Australian Journal of Chemistry, , vol. 43, # 2 p. 339 - 353
反应条件
ethanol; hydrazine hydrate Erwaermen des Reaktionsprodukts mit wss.Salzsaeure;
参考文献
Kornblum; Iffland
Journal of the American Chemical Society, 1949 , vol. 71, p. 2137,2138,2140
