您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
77152-08-0
合成路线
（共 108 条）
77152-08-0
+
38749-79-0
2-甲基-3-溴吡啶
→
反应条件
106877-18-3
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 60°C; 15 h; GloveboxSealed tube;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
2042-37-7
2-溴苯腈
+
77152-08-0
→
反应条件
447-60-9
2-三氟甲基苯腈
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23°C; 72 h; GloveboxSealed tube;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
77152-08-0
+
144025-03-6
2,4-二氟苯硼酸
→
反应条件
372-18-9
1,3-二氟苯
+
64248-61-9
2,4-二氟三氟甲基苯
反应条件
oxygen; triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide; toluene T=25°C; 4 h;
参考文献
Novak, Petr; Lishchynskyi, Anton; Grushin, Vladimir V.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 31 p. 7767 - 7770
10365-98-7
3-甲氧基苯硼酸
+
77152-08-0
→
反应条件
454-90-0
3-(三氟甲基)苯甲醚
反应条件
oxygen; triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide; toluene T=25°C; 4.5 h;
参考文献
Novak, Petr; Lishchynskyi, Anton; Grushin, Vladimir V.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 31 p. 7767 - 7770
766-85-8
3-碘苯甲醚
+
77152-08-0
→
反应条件
454-90-0
3-(三氟甲基)苯甲醚
反应条件
triethylamine tris(hydrogen fluoride) T=23 - 50°C; 48 h; GloveboxSealed tube; TemperatureTime;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
696-41-3
3-碘苯甲醛
+
77152-08-0
→
反应条件
454-89-7
3-三氟甲基苯甲醛
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 42 h; GloveboxSealed tube; TemperatureTime;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
2005-43-8
2-溴喹啉
+
77152-08-0
→
反应条件
347-42-2
2-三氟甲基喹啉
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23°C; 48 h; Inert atmosphere; TemperatureTime;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
51934-41-9
对碘苯甲酸乙酯
+
77152-08-0
→
反应条件
583-02-8
4-(三氟甲基)苯甲酸乙酯
反应条件
triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=23 - 50°C; 42 h; Inert atmosphere; TemperatureTime;
参考文献
Lishchynskyi, Anton; Novikov, Maxim A.; Martin, Eddy; Escudero-Adan, Eduardo C.; Novak, Petr; Grushin, Vladimir V.
Journal of Organic Chemistry, 2013 , vol. 78, # 22 p. 11126 - 11146
4334-88-7
4-乙氧羰基苯硼酸
+
77152-08-0
→
反应条件
583-02-8
4-(三氟甲基)苯甲酸乙酯
反应条件
oxygen; triethylamine tris(hydrogen fluoride) in N,N-dimethyl-formamide T=25°C; 0.5 h;
参考文献
Novak, Petr; Lishchynskyi, Anton; Grushin, Vladimir V.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 31 p. 7767 - 7770
77152-08-0
+
94-09-7
苯佐卡因
→
反应条件
583-02-8
4-(三氟甲基)苯甲酸乙酯
反应条件
1: 4-amino-benzoic acid ethyl ester With hydrogenchloride in water T=0°C; 0.0833333 h; Inert atmosphereSchlenk technique; 2: With sodium nitrite T=0°C; 0.25 h; Inert atmosphereSchlenk technique; 3: trifluoromethylcopper(I) T=0 - 20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Xi; Xu, Yan; Mo, Fanyang; Ji, Guojing; Qiu, Di; Feng, Jiajie; Ye, Yuxuan; Zhang, Songnan; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2013 , vol. 135, # 28 p. 10330 - 10333
1
2
3
4
...
11
下一页
末页
到第
页
确定
