in DMF-d7
byproducts: (CH3)3COH, KCl; (Ar); addn. of fluoroform to mixt. of copper chloride and potassium tert-butoxide in DMF-d7 at room temp.; NMR monitoring;
参考文献
Zanardi, Alessandro; Novikov, Maxim A.; Martin, Eddy; Benet-Buchholz, Jordi; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 51 p. 20901 - 20913
in N,N-dimethyl-formamide
byproducts: (CH3)3COH, NaCl; (Ar); reaction of copper chloride with 2 equiv. of sodium tert-butoxide in DMF, addn. of fluoroform; NMR monitoring;
参考文献
Zanardi, Alessandro; Novikov, Maxim A.; Martin, Eddy; Benet-Buchholz, Jordi; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 51 p. 20901 - 20913
