Fowles, G. W. A.; Lanigan, P. G.; Nicholls, D.
Chemistry and Industry (London, United Kingdom), 1961 , p. 1167 - 1168
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Gmelin Handbook: V: MVol.B1, 77, page 210 - 213
in neat (no solvent) heating 4 h at 700°C at light red heat;; pptn.;;
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Gmelin Handbook: V: MVol.B1, 84, page 227 - 230
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反应条件
in neat (no solvent) heating in quartz tube under high vac. at 720°C about 1 - 2 h;; removal of VCl4 and VOCl3 in vac.; extn. of VCl2 and excess of VCl3 with dimethyl formamide; pptn. washing with EtOH and ether, drying in vac.;;
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Schaefer, H.; Wartenpfuhl, F.
Journal of the Less-Common Metals, 1961 , vol. 3, p. 29 - 33
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Gmelin Handbook: V: MVol.B1, 84, page 227 - 230