暂无反应条件数据

aluminium trichloride in not given Si-compound reacted with GeCl4 in presence of AlCl3 at 110-120°C for 3 h;

C6H5MgBr in not given

暂无反应条件数据

T=550 - 600°C;

T=575°C;

magnesium 1) THF; 2) ether, first 12 h at 20 deg C then 3 h, reflux; Yield given. Multistep reaction;

暂无反应条件数据

SbF3

1: 78 percent / petroleum ether / 1.) reflux, 3 h, 2.) room temp., 12 h 2: 88 percent / n-BuLi / tetrahydrofuran; hexane / 2 h / 55 °C 3: 91 percent / 5 h / Heating 4: 1.) Mg / 1.) ether, 2.) ether, 20 deg C, 3 h; reflux, 12 h 5: 80 percent / acetonitrile / 1.) reflux, 3 h, 2.) 20 deg C, 12 h 6: 77 percent / aq. ethanol / 22 h / 20 °C View Scheme