in neat (no solvent) molar ratio rhenium telluride/PCl5 1/8; heated in evacuated sealed ampoules for 6 h at 170°C, cooled; PCl3 removed in a vac. at 80°C, extd. with hot monoglyme, soln. cooled, resulting crystals filtered off, washed (CH3CN), dried in a vac.; elem.anal., NMR, mass spectra;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 32, p. 1049 - 1051
Zhurnal Neorganicheskoi Khimii, , vol. 32, p. 1769 - 1771