2-苯基-1,3-二恶烷合成路线 （共 72 条）
反应条件
1: 94 percent / LAH/AlCl3 / diethyl ether / 2 h / Ambient temperature 2: PCC / CH2Cl2 / 2 h View Scheme
参考文献
Mittendorf, John; Hiemstra, Henk; Speckamp, W. Nico
Tetrahedron, 1990 , vol. 46, # 11 p. 4049 - 4062
反应条件
orthoformic acid triethyl ester; zirconium tetrachloride in dichloromethane
0.416667 h; Ambient temperature;
参考文献
Gregg, Brian T.; Golden, Kathryn C.; Quinn, John F.
Tetrahedron, 2008 , vol. 64, # 15 p. 3287 - 3295
反应条件
indium trifluoromethanesulfonate in dichloromethane
T=20°C; 0.5 h;
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 6.5 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
N-bromosuccinmide in dichloromethane
T=20°C; 0.0833333 h;
参考文献
Karimi, Babak; Seradj, Hassan; Maleki, Jafar
Tetrahedron, 2002 , vol. 58, # 22 p. 4513 - 4516
反应条件
PTAB; N-benzyl-N,N,N-triethylammonium chloride; antimony(III)tribromide in dimethyl sulfoxide
T=20°C; 70 h;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
sodium hydrogen sulphate; silica gel in dichloromethane
T=20°C; 0.166667 h;
参考文献
Das, Biswanath; Ramu, Ravirala; Reddy, Majjigapu Ravinder; Mahender, Gurram
Synthesis, 2005 , # 2 art. no. P10504SS, p. 250 - 254
反应条件
PTAB; N-benzyl-N,N,N-triethylammonium chloride; antimony(III)tribromide in dimethyl sulfoxide
T=20°C; 70 h;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
