2-苯基-1,3-二恶烷合成路线 （共 72 条）
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide
T=20°C;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide
T=55°C; 2 h;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide
T=20°C;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
tungsten hexachloride; orthoformic acid triethyl ester in dichloromethane
0.0833333 h; Ambient temperature;
参考文献
Firouzabadi; Iranpoor; Karimi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2255 - 2263
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
T=-5 - 0°C; 1.5 h;
参考文献
Barbasiewicz, Michal; Makosza, Mieczyslaw
Organic Letters, 2006 , vol. 8, # 17 p. 3745 - 3748
反应条件
potassium tert-butylate in N,N-dimethyl-formamide
T=-60°C; 1.5 h;
参考文献
Barbasiewicz, Michal; Makosza, Mieczyslaw
Organic Letters, 2006 , vol. 8, # 17 p. 3745 - 3748
反应条件
tungsten hexachloride; orthoformic acid triethyl ester in dichloromethane
0.266667 h; Ambient temperature;
参考文献
Firouzabadi; Iranpoor; Karimi
Synthetic Communications, 1999 , vol. 29, # 13 p. 2255 - 2263
反应条件
trimethylsilyl trifluoromethanesulfonate in tetrahydrofuran
T=-78 - 0°C;
参考文献
Hunter, Roger; Michael, Joseph P.; Tomlinson, Geoffrey D.
Tetrahedron, 1994 , vol. 50, # 3 p. 871 - 888
反应条件
toluene-4-sulfonic acid
参考文献
Bailey, William F.; Croteau, Allan A.
Tetrahedron Letters, 1981 , vol. 22, p. 545 - 548
反应条件
1: 95 percent / NaHSO4*SiO2 / CH2Cl2 / 0.08 h / 20 °C
2: 83 percent / NaHSO4*SiO2 / CH2Cl2 / 0.17 h / 20 °C
View Scheme
参考文献
Das, Biswanath; Ramu, Ravirala; Reddy, Majjigapu Ravinder; Mahender, Gurram
Synthesis, 2005 , # 2 art. no. P10504SS, p. 250 - 254
