3,5-二甲基-1H-吡唑-1-胺合成路线 （共 17 条）
反应条件
iodine cloride in dichloromethane
1 h; Ambient temperature;
参考文献
Ohsawa, Akio; Kaihoh, Terumitsu; Itoh, Takashi; Okada, Mamiko; Kawabata, Chikako; et al.
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 10 p. 3838 - 3848
反应条件
N-chloro-succinimide in dichloromethane
3 h; Ambient temperature;
参考文献
Ohsawa, Akio; Kaihoh, Terumitsu; Itoh, Takashi; Okada, Mamiko; Kawabata, Chikako; et al.
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 10 p. 3838 - 3848
反应条件
lithium perchlorate in acetonitrile
electrochemical oxidation, Pt-electrode; dependence of product yield and distribution on addition of H2O or pyridine as solvents; same reaction of further N-aminopyrazoles; Product distributionMechanism;
参考文献
Itoh; Nagata; Okada; Ohsawa
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 6 p. 1524 - 1526
反应条件
N-chloro-succinimide in dichloromethane
1 h; Ambient temperature;
参考文献
Ohsawa, Akio; Kaihoh, Terumitsu; Itoh, Takashi; Okada, Mamiko; Kawabata, Chikako; et al.
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, # 10 p. 3838 - 3848
反应条件
1: 58 percent / lead tetra-acetate / CH2Cl2 / 0 °C
2: 20 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Ohsawa, Akio; Arai, Heihachiro; Ohnishi, Hidefumi; Igeta, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1980 , # 24 p. 1182 - 1183
反应条件
1: 58 percent / lead tetra-acetate / CH2Cl2 / 0 °C
2: 48 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Ohsawa, Akio; Arai, Heihachiro; Ohnishi, Hidefumi; Igeta, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1980 , # 24 p. 1182 - 1183
反应条件
1: 58 percent / lead tetra-acetate / CH2Cl2 / 0 °C
2: 48 percent / m-chloroperbenzoic acid / CH2Cl2 / Ambient temperature
3: H2 / Pd-C
View Scheme
参考文献
Ohsawa, Akio; Arai, Heihachiro; Ohnishi, Hidefumi; Igeta, Hiroshi
Journal of the Chemical Society, Chemical Communications, 1980 , # 24 p. 1182 - 1183
