7-氯-2,4-二甲基-[1,8]萘啶合成路线 （共 9 条）
反应条件
n-butyllithium 1) hexane, THF, 15 min, 2) 4 h; Yield given. Multistep reaction;
参考文献
Grassi, Maria; Munno, Giovanni De; Nicolo, Francesco; Schiavo, Sandra Lo
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1992 , # 15 p. 2367 - 2374
参考文献
Ochiai; Miyaki
Chemische Berichte, 1941 , vol. 74, p. 1115,1123
Show Details
Miyaki
Yakugaku Zasshi, 1942 , vol. 62, p. 26,35
Chem.Abstr., 1951 , p. 627
反应条件
1: H2O / Diazotization
2: POCl3
View Scheme
参考文献
Ochiai; Miyaki
Chemische Berichte, 1941 , vol. 74, p. 1115,1123
Show Details
Miyaki
Yakugaku Zasshi, 1942 , vol. 62, p. 26,35
Chem.Abstr., 1951 , p. 627
反应条件
1: concentrated H2SO4
2: H2O / Diazotization
3: POCl3; PCl5
View Scheme
参考文献
Mangini; Colonna
Gazzetta Chimica Italiana, 1943 , vol. 73, p. 323,327
反应条件
1: concentrated H2SO4
2: H2O / Diazotization
3: POCl3; PCl5
View Scheme
参考文献
Mangini; Colonna
Gazzetta Chimica Italiana, 1943 , vol. 73, p. 323,327
反应条件
1: sulfuric acid; sodium nitrite
2: trichlorophosphate / |Reflux
View Scheme
参考文献
Shi, Yong Gang; Duan, Yu Lian; Chen, Jian Hua; Wu, Xiang Hua; Zhou, Ying; Zhang, Jun Feng
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 63 - 67
反应条件
trichlorophosphate
Reflux;
参考文献
Shi, Yong Gang; Duan, Yu Lian; Chen, Jian Hua; Wu, Xiang Hua; Zhou, Ying; Zhang, Jun Feng
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 63 - 67
反应条件
potassium hydroxide; palladium on activated charcoal
Hydrogenation;
参考文献
Ochiai; Miyaki
Chemische Berichte, 1941 , vol. 74, p. 1115,1123
Full Text Show Details
Miyaki
Yakugaku Zasshi, 1942 , vol. 62, p. 26,35
Chem.Abstr., 1951 , p. 627
参考文献
Ferrarini; Mori; Biagi; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 2 p. 417 - 419
