(2-氨基-5-硝基苯基)甲醇合成路线 （共 13 条）
反应条件
sulfuric acid; copper(II) sulfate Diazotization.auf dem Dampfbad;
参考文献
Fourneau; de Lestrange
Bulletin de la Societe Chimique de France, 1933 , vol. <4> 53, p. 330,332
反应条件
borane-THF in tetrahydrofuran
T=0 - 30°C; 23 h; Inert atmosphere;
参考文献
The Procter and Gamble Company; GARDLIK, John Michael; PATTEN, Monica Jo; GARRETT, Garry Steven; MURPHY, Bryan Patrick
Patent: US2014/121415 A1, 2014 ;
Location in patent: Paragraph 0050 ;
反应条件
sodium tetrahydroborate; sodium hydroxide in ethanol
T=0 - 18°C; 3.41667 h; Inert atmosphereCooling with ice;
参考文献
The Procter and Gamble Company; GARDLIK, John Michael; PATTEN, Monica Jo; GARRETT, Garry Steven; MURPHY, Bryan Patrick
Patent: US2014/121414 A1, 2014 ;
Location in patent: Paragraph 0045 ;
反应条件
hydrogenchloride; sodium borohydride in ethanol
参考文献
Imperial Chemical Industries Limited
Patent: US4268510 A1, 1981 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 10°C;
参考文献
Shankar; Wagh, Manoj Balu; Madhubabu; Vembu; Kumar, U. K. Syam
Synlett, 2011 , # 6 p. 844 - 848
反应条件
sulfuric acid; nitric acid
T=0°C; anschliessend Erwaermen des Reaktionsprodukts mit wss.-aethanol. Natronlauge. Die Konstitution des Praeparats ist ungewiss.;
参考文献
Fourneau; de Lestrange
Bulletin de la Societe Chimique de France, 1933 , vol. <4> 53, p. 330,332
反应条件
1: nitric acid / acetic acid / 4.58 h / 38 - 44 °C
2: sodium tetrahydroborate; sodium hydroxide / ethanol / 3.42 h / 0 - 18 °C / |Inert atmosphere; |Cooling with ice
View Scheme
参考文献
The Procter and Gamble Company; GARDLIK, John Michael; PATTEN, Monica Jo; GARRETT, Garry Steven; MURPHY, Bryan Patrick
Patent: US2014/121414 A1, 2014 ;
反应条件
potassium hydroxide
T=0°C;
参考文献
Niyogy
Journal of the Indian Chemical Society, 1931 , vol. 8, p. 59,65
反应条件
1: sodium acetate
2: sulfuric acid; nitric acid / 0 °C / anschliessend Erwaermen des Reaktionsprodukts mit wss.-aethanol. Natronlauge. Die Konstitution des Praeparats ist ungewiss.
View Scheme
参考文献
Fourneau; de Lestrange
Bulletin de la Societe Chimique de France, 1933 , vol. <4> 53, p. 330,332
反应条件
calcium chloride; zinc
参考文献
Fourneau; de Lestrange
Bulletin de la Societe Chimique de France, 1933 , vol. <4> 53, p. 330,332
