(2-氨基-5-硝基苯基)甲醇合成路线 (共 13 条)
反应条件
1: trifluoroacetic acid / 72 °C
2: palladium 10 on activated carbon; ammonium formate / methanol / Reflux
View Scheme
参考文献
Shankar; Wagh, Manoj Balu; Madhubabu; Vembu; Kumar, U. K. Syam
Synlett, 2011 , # 6 p. 844 - 848
反应条件
in 1,4-dioxane
T=20°C;
参考文献
PFIZER PRODUCTS INC.
Patent: WO2007/93904 A1, 2007 ;
Location in patent: Page/Page column 24 ;
反应条件
manganese(IV) oxide in dichloromethane
T=20°C; 23 h; Inert atmosphere;
参考文献
Ida, Yoshihiro; Matsubara, Ayaka; Nemoto, Toru; Saito, Manabu; Hirayama, Shigeto; Fujii, Hideaki; Nagase, Hiroshi
Bioorganic and Medicinal Chemistry, 2012 , vol. 20, # 19 p. 5810 - 5831