1,5-二异丙基-2,4-二硝基苯合成路线 (共 6 条)
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
sodium tetrahydroborate; water; palladium on activated charcoal 1 h; Ambient temperature;
参考文献
Beak, Peter; Carter, Linda G.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2363 - 2373
反应条件
T=60°C; Hydrogenation;
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
trifluorormethanesulfonic acid; nitric acid in dichloromethane
1.) 25 deg C, 1 h, 2.) 30-38 deg C, 0.5 h;
参考文献
Beak, Peter; Carter, Linda G.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2363 - 2373
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1: 86 percent / NaBH4, H2O / 10percent Pd/C / 1 h / Ambient temperature
2: 83 percent / pyridinium perbromide, pyridine / tetrahydrofuran / 2 h / -70 °C
View Scheme
参考文献
Beak, Peter; Carter, Linda G.
Journal of Organic Chemistry, 1981 , vol. 46, # 11 p. 2363 - 2373