in benzene Electrochem. Process; precipitation of Al, no Li;;
参考文献
Plotnikov, V. A.; Shcheka, I. A.; Jankelevich, V. A.
Zhurnal obshchei Khim. (russ.), 1933 , vol. 3, p. 481 - 499
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Gmelin Handbook: Li: SVol., 32, page 205 - 207
in hexane byproducts: LiBr; (under Ar); solns. of alane-compd. and Al2Br6 in hexane are combined and kept at 80°C for 2 h; filtn., volatiles were removed by distn., residue was recrystd. from n-pentane, identified by NMR.;
参考文献
Uhl, W.; Schnepf, J. E. O.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1991 , vol. 595, p. 225 - 238
in neat (no solvent) byproducts: CBrCl3; AlBr3 evacuated in flask; cooled with liq. N2; CFCl3 (6 equiv.) condensed on the solid; warmed up to 200 K; stirred for 1 h; warmed to room temp.; refluxed for one more hour; liq. evapd. in vac.;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 48 p. 6653 - 6656
