三氯一氧化钒 三氯代氧化钒(V)合成路线 （共 117 条）
参考文献
Journal of thermal analysis, , vol. 35, # 1 p. 163 - 173
参考文献
Journal of thermal analysis, , vol. 35, # 1 p. 163 - 173
反应条件
in gas byproducts: Cl2; Irradiation (UV/VIS); irradiation of VOCl3 by pulsed CO2 laser radiation; detected by luminescence spectroscopy;
参考文献
Sausa, R. C.; Ronn, A. M.
Journal of Chemical Physics, 1984 , vol. 81, # 4 p. 1716 - 1724
反应条件
in dichloromethane byproducts: (CH3)3SiCl; (N2); addn. of 2 equiv. of silane deriv. to CH2Cl2 soln. of vanadium compd. at room temp., stirring for 2 h at room temp.; evapn., elem. anal.;
参考文献
Romero-Fernandez, Javier; Carrillo-Hermosilla, Fernando; Antinolo, Antonio; Alonso-Moreno, Carlos; Rodriguez, Ana M.; Lopez-Solera, Isabel; Otero, Antonio
Dalton Transactions, 2010 , vol. 39, # 28 p. 6419 - 6425
反应条件
in chloroform-d1 in the presence of MS4A molecular sieve, there is no reaction in the presence of collidine;
参考文献
Hirao, Toshikazu; Mori, Makoto; Ohshiro, Yoshiki
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 7 p. 2399 - 2400
反应条件
in tetrachloromethane
参考文献
Gmelin Handbook: V: MVol.B1, 91, page 246 - 247
反应条件
in diethyl ether; hexane addn. of a soln. of VOCl3 in ether to a suspension of LiOSiPh3 in n-hexane with stirring and refluxing in absence of moisture; refluxing for 1 h;; filtration after cooling; the residue was washed with ether and extracted with warm toluene for several times; evapn.; dried; elem. anal.;;
参考文献
Preuss, Fritz; Noichl, Harald
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1987 , vol. 42, # 2 p. 121 - 129
反应条件
hydrogen in neat (no solvent) reaction by thermic decompn. of VOCl3 on a Pt- or W wire, heated up to white heat, in presence of H2;; formation of metallic V;;
参考文献
Edson, R.; McIntosh, D.
Trans. R. Soc. Can., 1915 , vol. 9, p. 81 - 83
反应条件
hydrogen in neat (no solvent) at 850°C;;
参考文献
McCarley, R. E.; Roddy, J. W.
IS-17 (1959) 31/4
反应条件
in neat (no solvent) heating reagents;;
参考文献
Journal of the American Chemical Society, , vol. 79, p. 326
Journal of the American Chemical Society, , vol. 79, p. 4913
