三氯一氧化钒 三氯代氧化钒(V)合成路线 （共 117 条）
反应条件
in not given byproducts: VOCl, H2; reflux;;
参考文献
Journal of the American Chemical Society, , vol. 79, p. 4913
Sn: Org.Verb.4, 1.2.1.1.2.4.3, page 31 - 32
反应条件
in hexane under Ar; 41 mmol ZnMes2 added to 82 mmol VOCl3 in hexane at -20°C; mixt. stirred at room temp. for 2-3 h; dark-blue ppt. (VOCl2*ZnCl2) filtered off; filtrate concd. and cooled; elem. anal.;
参考文献
Seidel, W.; Kreisel, G.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 559, p. 118 - 122
反应条件
in neat (no solvent) pptn.;;
参考文献
Ehrlich, P.; Engel, W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1963 , vol. 322, p. 217 - 223
Full Text Show Details
Gmelin Handbook: V: MVol.B1, 90, page 243 - 246
反应条件
in neat (no solvent) mixing of MgO with VOCl3 in quartz reactor; heating under He at 723 K for 3 h; monitoring by XRD and IR;
参考文献
Tamai, Tsukasa; Inazu, Koji; Aika, Ken-Ichi
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 8 p. 1565 - 1574
反应条件
in neat (no solvent) at -180°C;;
参考文献
Gmelin Handbook: V: MVol.B1, 91, page 246 - 247
反应条件
in tetrachloromethane at 5°C;;
参考文献
Schmeisser, M.
Angewandte Chemie, 1955 , vol. 67, p. 493 - 501
Full Text Show Details
Gmelin Handbook: V: MVol.B1, 90, page 243 - 246
参考文献
Gmelin Handbook: V: MVol.B1, 91, page 246 - 247
反应条件
in neat (no solvent) heating reagents;;
参考文献
Gmelin Handbook: V: MVol.B1, 91, page 246 - 247
反应条件
in neat (no solvent) heating under inflammation;;
参考文献
Roscoe, H. E.
Justus Liebigs Annalen der Chemie, 1868 , vol. 6, p. 77 - 116
Full Text Show Details
Roscoe, H. E.
Philosophical Transactions of the Royal Society of London, 1868 , vol. 158, p. 1 - 27
反应条件
sugar coal in neat (no solvent)
参考文献
Gmelin Handbook: V: MVol.B1, 90, page 243 - 246
