2,4,6-三甲基吡喃鎓四氟硼酸盐合成路线 (共 19 条)
反应条件
tetrafluoroboric acid T=100°C; 0.5 h;
参考文献
Bulletin de la Societe Chimique de France, , # 1 p. 205 - 211
反应条件
tetrafluoroboric acid T=80 - 100°C; Cycloaddition;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 43, # 6 p. 565 - 583
反应条件
boron trifluoride diethyl etherate
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 19, # 4 p. 364 - 368
Khimiya Geterotsiklicheskikh Soedinenii, , # 4 p. 454 - 458
反应条件
tetrafluoroboric acid; diethyl ether; acetic acid; methoxybenzene
参考文献
Justus Liebigs Annalen der Chemie, , vol. 618, p. 140,148
Org. Synth. Coll. Vol. V, <1973> 1108
反应条件
triethylamine in acetonitrile T=-40°C; 6 h;
参考文献
Vernaudon, Pascal; Rajoharison, Harivelo G.; Roussel, Chritian
Bulletin de la Societe Chimique de France, 1987 , # 1 p. 205 - 211
反应条件
in methanol 12 h; Heating;
参考文献
Rippert, Andreas Johannes; Hansen, Hans Juergen
Helvetica Chimica Acta, 1995 , vol. 78, p. 238 - 241
反应条件
sodium 1.) THF, 25-42 deg C, 40 min, 2.) THF, 25 deg C, 20 min; Yield given. Multistep reaction;
参考文献
Fallahpour, Reza-Ali; Hansen, Hans-Juergen
Helvetica Chimica Acta, 1995 , vol. 78, # 6 p. 1419 - 1436
反应条件
sodium dihydrogenphosphate; dihydrogen peroxide in water T=100°C; 0.333333 h;
参考文献
Balaban, Teodor Silviu; Hiegemann, Monika
Tetrahedron, 1992 , vol. 48, # 45 p. 9827 - 9840
参考文献
Garst, Michael E.; Frazier, Janice D.
Journal of Organic Chemistry, 1982 , vol. 47, # 18 p. 3553 - 3556
反应条件
in tetrahydrofuran; dimethyl sulfoxide 1.) -5 deg C, 1 h, 2.) room temperature, 7 h;
参考文献
Garst, Michael E.; Frazier, Janice D.
Journal of Organic Chemistry, 1982 , vol. 47, # 18 p. 3553 - 3556