2,4,6-三甲基吡喃鎓四氟硼酸盐合成路线 （共 19 条）
参考文献
Heterocycles, , vol. 16, # 1 p. 17 - 20
反应条件
triethylamine in acetonitrile T=-40°C; 6 h;
参考文献
Vernaudon, Pascal; Rajoharison, Harivelo G.; Roussel, Chritian
Bulletin de la Societe Chimique de France, 1987 , # 1 p. 205 - 211
反应条件
triethylamine in acetonitrile T=-40°C; 6 h;
参考文献
Bulletin de la Societe Chimique de France, , # 1 p. 205 - 211
反应条件
ammonium hydroxide 3 h; Ambient temperature; Yield given;
参考文献
Winter, Arthur H.; Gibson, Harry H.; Falvey, Daniel E.
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8186 - 8195
反应条件
in tetrahydrofuran; diethyl ether T=-78 - 20°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yamamoto, Yohsuke; Kume, Takashi; Akiba, Kin-ya
Heterocycles, 1987 , vol. 26, # 6 p. 1495 - 1498
反应条件
hydrogen; palladium on activated charcoal 1.) THF, ether, from -78 deg C to RT, 2.) ethanol; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Yamamoto, Yohsuke; Kume, Takashi; Akiba, Kin-ya
Heterocycles, 1987 , vol. 26, # 6 p. 1495 - 1498
反应条件
sodium dihydrogenphosphate; dihydrogen peroxide in water
T=100°C; 0.333333 h;
参考文献
Balaban, Teodor Silviu; Hiegemann, Monika
Tetrahedron, 1992 , vol. 48, # 45 p. 9827 - 9840
反应条件
1: 35 percent / tetrahydrofuran / 45 deg C then r.t., 1 h
2: 100 percent / LiAlH4 / diethyl ether / 0.5 h / 0 °C
3: 67 percent / MnO2 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Briquet, Anne Andree Sophie; Hansen, Hans-Juergen
Helvetica Chimica Acta, 1994 , vol. 77, p. 1921 - 1939
反应条件
triethylamine in acetonitrile
T=-40°C; 6 h;
参考文献
Vernaudon, Pascal; Rajoharison, Harivelo G.; Roussel, Chritian
Bulletin de la Societe Chimique de France, 1987 , # 1 p. 205 - 211
