1,2,2-三氟-2-羟基-1-三氟甲基乙烷磺酸合成路线 （共 25 条）
反应条件
silver fluoride
1.) diglyme, 3h, 35-39 deg C, 2.) 35-38 deg C, 3 d; Yield given. Multistep reaction;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 3 p. 331 - 347
反应条件
silver fluoride
1.) diglyme, 2h, 35 deg C, 2.) 35-37 deg C, 3 d; Yield given. Multistep reaction;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 3 p. 331 - 347
反应条件
silver fluoride
1.) diglyme, 3h, 30-35 deg C, 2.) 30-32 deg C, 48 h; Yield given. Multistep reaction;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 49, # 3 p. 331 - 347
参考文献
Ragulin, L. N.; Ropalo, P. P.; Sokol'skii, G. A.; Knunyants, I. L.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1685 - 1688
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1754 - 1758
C.A., 1968 , vol. 68, p. 48977
Full Text Show Details
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
反应条件
sulfuric acid
100 percent H2SO4 used, 270-280°C, 6-8 h, in auto clave;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.3.2, page 99 - 119
