5,7-二氯-8-羟基喹啉合成路线 （共 13 条）
反应条件
1: potassium carbonate; tetrabutylammomium bromide / methanol; water; dichloromethane / 68 h / 20 °C 2: β-glucosidase from almonds; water / aq. phosphate buffer / 0.67 h / 37 °C / pH 7.4 / |Enzymatic reaction View Scheme
参考文献
Oliveri, Valentina; Viale, Maurizio; Caron, Giulia; Aiello, Cinzia; Gangemi, Rosaria; Vecchio, Graziella
Dalton Transactions, 2013 , vol. 42, # 6 p. 2023 - 2034
反应条件
potassium carbonate; potassium iodide; 2-chloro-acetamide in N,N-dimethyl-formamide T=90 - 150°C; Smiles Aromatic Rearrangement; 4 h; Reagent/catalyst;
参考文献
Xie, Yong-Sheng; Vijaykumar; Jang, Kiwan; Shin, Hong-Hyun; Zuo, Hua; Shin, Dong-Soo
Tetrahedron Letters, 2013 , vol. 54, # 38 p. 5151 - 5154
反应条件
1: potassium carbonate; tetrabutylammomium bromide / methanol; water; dichloromethane / 68 h / 20 °C 2: β-glucosidase from almonds; water / aq. phosphate buffer / 0.67 h / 37 °C / pH 7.4 / |Enzymatic reaction View Scheme
参考文献
Oliveri, Valentina; Viale, Maurizio; Caron, Giulia; Aiello, Cinzia; Gangemi, Rosaria; Vecchio, Graziella
Dalton Transactions, 2013 , vol. 42, # 6 p. 2023 - 2034
