1: With trimethylaluminum; ammonium chloride in toluene T=80°C; Garigipati's reaction; 48 h; Inert atmosphere; 2: With silica gel in methanol; chloroform 1 h;
参考文献
Wang, Lei; Moss, Robert A.; Krogh-Jespersen, Karsten
Journal of Physical Chemistry A, 2011 , vol. 115, # 28 p. 8113 - 8118
in toluene
under dry Ar; pentafluorobenzonitrile added via syringe to a soln. of Ge-compd. in dry toluene, refluxed 12h; evapn. (vac.), crystn. (acetonitrile), elem. anal.;
参考文献
Katti, K. V.; Batchelor, R. J.; Einstein, F. W. B.; Cavell, R. G.
Inorganic Chemistry, 1990 , vol. 29, p. 808 - 814