2-甲基-1-(苯基甲基)吖丁啶合成路线 （共 3 条）
反应条件
n-butyllithium in tetrahydrofuran
T=20°C; 2 h; Inert atmosphere;
参考文献
Kenis, Sara; D'Hooghe, Matthias; Verniest, Guido; Dang Thi, Tuyet Anh; Pham The, Chinh; Van Nguyen, Tuyen; De Kimpe, Norbert
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5982 - 5992
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
2: n-butyllithium / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Kenis, Sara; D'Hooghe, Matthias; Verniest, Guido; Dang Thi, Tuyet Anh; Pham The, Chinh; Van Nguyen, Tuyen; De Kimpe, Norbert
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5982 - 5992
反应条件
1: methanol / 72 h / Reflux
2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Reflux
3: n-butyllithium / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Kenis, Sara; D'Hooghe, Matthias; Verniest, Guido; Dang Thi, Tuyet Anh; Pham The, Chinh; Van Nguyen, Tuyen; De Kimpe, Norbert
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5982 - 5992
