Boc-L-2-氨基己二酸合成路线 （共 10 条）
反应条件
triethylamine in water; N,N-dimethyl-formamide 1 h;
参考文献
De Cat, Inge; Gobbo, Cristian; Van Averbeke, Bernard; Lazzaroni, Roberto; De Feyter, Steven; Van Esch, Jan
Journal of the American Chemical Society, 2011 , vol. 133, # 51 p. 20942 - 20950
反应条件
sodium hydroxide in methanol T=20°C; 1 h;
参考文献
Sakura, Naoki; Hirose, Kyoko; Hashimoto, Tadashi
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 8 p. 3506 - 3509
反应条件
sodium hydroxide in methanol T=20°C; 1 h;
参考文献
Sakura, Naoki; Hirose, Kyoko; Hashimoto, Tadashi
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 8 p. 3506 - 3509
反应条件
sodium hydroxide in methanol T=20°C; 1 h;
参考文献
Sakura, Naoki; Hirose, Kyoko; Hashimoto, Tadashi
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 8 p. 3506 - 3509
反应条件
sodium hydroxide; nickel 1) dioxane, room temperature, 1h, 2) ethanol, room temperature; Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 43, # 19 p. 4297 - 4308
反应条件
1: 1) N-methyl morpholine, isobutyl chloroformate, 2) triethylamine / 1) THF, -15 deg C, 5 min, 2) THF, -15 deg C, 45 min, in the dark 2: 0.33 h / Ambient temperature; Irradiation 3: 1) 1N aqueous sodium hydroxide, / 2) Raney Ni / 1) dioxane, room temperature, 1h, 2) ethanol, room temperature View Scheme
参考文献
Tetrahedron, , vol. 43, # 19 p. 4297 - 4308
反应条件
1: 0.33 h / Ambient temperature; Irradiation 2: 1) 1N aqueous sodium hydroxide, / 2) Raney Ni / 1) dioxane, room temperature, 1h, 2) ethanol, room temperature View Scheme
参考文献
Tetrahedron, , vol. 43, # 19 p. 4297 - 4308
反应条件
1: 1.) ruthenium tetroxide; 2.) zinc / 2.) acetic acid 2: 91 percent / 1 N sodium hydroxide / methanol / 1 h / 20 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 34, # 8 p. 3506 - 3509
反应条件
sodium tetrahydroborate; iodine in tetrahydrofuran T=0 - 20°C; 1.16667 h;
参考文献
Matsumoto, Naoki; Kaneko, Katsura; Nagai, Hazuki; Konuki, Kaname; Tsuchida, Toshio; Issiki, Kunio
Patent: US2004/249205 A1, 2004 ;
Location in patent: Page 3 ;
反应条件
trifluoroacetic acid in dichloromethane 1 h; Ambient temperature;
参考文献
Barton; Herve; Potier; Thierry
Tetrahedron, 1987 , vol. 43, # 19 p. 4297 - 4308
