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63148-62-9
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
773060-41-6
合成路线
（共 8 条）
606098-82-2
→
反应条件
773060-41-6
反应条件
1: CuI / Pd(PPh3)4 / various solvent(s) / 12 h 2: (C4H9)4NF / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Lehmann, Matthias; Kang, Shin-Woong; Koehn, Christiane; Haseloh, Soenke; Kolb, Ute; Schollmeyer, Dieter; Wang, Qingbing; Kumar, Satyendra
Journal of Materials Chemistry, 2006 , vol. 16, # 44 p. 4326 - 4334
773060-37-0
→
反应条件
773060-41-6
反应条件
1.1: CuI / Pd(PPh3)4 / various solvent(s) 1.2: CuI / Pd(PPh3)4 / various solvent(s) 1.3: 92 percent / K2CO3 / methanol; tetrahydrofuran 2.1: CuI / Pd(PPh3)4 / various solvent(s) / 12 h 3.1: (C4H9)4NF / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Lehmann, Matthias; Kang, Shin-Woong; Koehn, Christiane; Haseloh, Soenke; Kolb, Ute; Schollmeyer, Dieter; Wang, Qingbing; Kumar, Satyendra
Journal of Materials Chemistry, 2006 , vol. 16, # 44 p. 4326 - 4334
25245-34-5
1-溴-2,5-二甲氧基苯
→
反应条件
773060-41-6
反应条件
1.1: 84 percent / iodine; KIO3; sulfuric acid / CCl4; acetic acid / 5 h / 80 °C 2.1: 77 percent / BBr3 / CH2Cl2 / 1 h / 20 °C 3.1: 82 percent / KOH / dimethylformamide / 3 h / 60 °C 4.1: CuI / Pd(PPh3)4 / various solvent(s) 4.2: CuI / Pd(PPh3)4 / various solvent(s) 4.3: 92 percent / K2CO3 / methanol; tetrahydrofuran 5.1: CuI / Pd(PPh3)4 / various solvent(s) / 12 h 6.1: (C4H9)4NF / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Lehmann, Matthias; Kang, Shin-Woong; Koehn, Christiane; Haseloh, Soenke; Kolb, Ute; Schollmeyer, Dieter; Wang, Qingbing; Kumar, Satyendra
Journal of Materials Chemistry, 2006 , vol. 16, # 44 p. 4326 - 4334
174518-82-2
→
反应条件
773060-41-6
反应条件
1.1: 77 percent / BBr3 / CH2Cl2 / 1 h / 20 °C 2.1: 82 percent / KOH / dimethylformamide / 3 h / 60 °C 3.1: CuI / Pd(PPh3)4 / various solvent(s) 3.2: CuI / Pd(PPh3)4 / various solvent(s) 3.3: 92 percent / K2CO3 / methanol; tetrahydrofuran 4.1: CuI / Pd(PPh3)4 / various solvent(s) / 12 h 5.1: (C4H9)4NF / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Lehmann, Matthias; Kang, Shin-Woong; Koehn, Christiane; Haseloh, Soenke; Kolb, Ute; Schollmeyer, Dieter; Wang, Qingbing; Kumar, Satyendra
Journal of Materials Chemistry, 2006 , vol. 16, # 44 p. 4326 - 4334
216306-47-7
→
反应条件
773060-41-6
反应条件
1.1: 82 percent / KOH / dimethylformamide / 3 h / 60 °C 2.1: CuI / Pd(PPh3)4 / various solvent(s) 2.2: CuI / Pd(PPh3)4 / various solvent(s) 2.3: 92 percent / K2CO3 / methanol; tetrahydrofuran 3.1: CuI / Pd(PPh3)4 / various solvent(s) / 12 h 4.1: (C4H9)4NF / tetrahydrofuran / 2 h / 20 °C View Scheme
参考文献
Lehmann, Matthias; Kang, Shin-Woong; Koehn, Christiane; Haseloh, Soenke; Kolb, Ute; Schollmeyer, Dieter; Wang, Qingbing; Kumar, Satyendra
Journal of Materials Chemistry, 2006 , vol. 16, # 44 p. 4326 - 4334
202798-00-3
→
反应条件
773060-41-6
反应条件
1: 66 percent / I2; KIO3; AcOH / CCl4 / Heating 2: piperidine; Pd(PPh3)4; CuI 3: K2CO3; methanol / tetrahydrofuran 4: piperidine; Pd(PPh3)4; CuI 5: tetrabutylammonium fluoride / tetrahydrofuran View Scheme
参考文献
Lehmann, Matthias; Levin, Jeremy
Molecular Crystals and Liquid Crystals, 2004 , vol. 411, p. 273/[1315]-281/[1323]
606098-81-1
→
反应条件
773060-41-6
反应条件
1: K2CO3; methanol / tetrahydrofuran 2: piperidine; Pd(PPh3)4; CuI 3: tetrabutylammonium fluoride / tetrahydrofuran View Scheme
参考文献
Lehmann, Matthias; Levin, Jeremy
Molecular Crystals and Liquid Crystals, 2004 , vol. 411, p. 273/[1315]-281/[1323]
6952-59-6
间溴苯腈
→
反应条件
773060-41-6
反应条件
1: piperidine; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) / 1 h / 65 °C 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h View Scheme
参考文献
Seltmann, Jens; Mueller, Kathrin; Klein, Susanne; Lehmann, Matthias
Chemical Communications, 2011 , vol. 47, # 23 p. 6680 - 6682
