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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
773092-53-8
合成路线
（共 5 条）
769100-08-5
7-(溴甲基)喹啉
→
反应条件
773092-53-8
反应条件
sodium azide in N,N-dimethyl-formamide T=75°C; 16 h;
参考文献
Cody, Wayne Livingston; Edmunds, Jeremy John; Holsworth, Daniel Dale; Powell, Noel Aaron
Patent: US2004/204455 A1, 2004 ;
Location in patent: Page/Page column 17 ;
39982-49-5
7-喹啉甲醇
→
反应条件
773092-53-8
反应条件
1: 100 percent / hydrobromic acid; acetic acid / 4 h / 70 °C 2: 99 percent / sodium azide / dimethylformamide / 16 h / 75 °C View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
346-55-4
4-氯-7-三氟甲基喹啉
→
反应条件
773092-53-8
反应条件
1.1: 90 percent / hydrogen; triethylamine / palladium on carbon / methanol 2.1: various solvent(s) / 2 h / 150 °C / cooling 2.2: 77 percent / Heating 3.1: 82 percent / REDAL / tetrahydrofuran; toluene / 4 h / -20 °C 4.1: 100 percent / hydrobromic acid; acetic acid / 4 h / 70 °C 5.1: 99 percent / sodium azide / dimethylformamide / 16 h / 75 °C View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
51552-68-2
喹啉-7-羧酸甲酯
→
反应条件
773092-53-8
反应条件
1: 82 percent / REDAL / tetrahydrofuran; toluene / 4 h / -20 °C 2: 100 percent / hydrobromic acid; acetic acid / 4 h / 70 °C 3: 99 percent / sodium azide / dimethylformamide / 16 h / 75 °C View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
325-14-4
7-三氟甲基喹啉
→
反应条件
773092-53-8
反应条件
1.1: various solvent(s) / 2 h / 150 °C / cooling 1.2: 77 percent / Heating 2.1: 82 percent / REDAL / tetrahydrofuran; toluene / 4 h / -20 °C 3.1: 100 percent / hydrobromic acid; acetic acid / 4 h / 70 °C 4.1: 99 percent / sodium azide / dimethylformamide / 16 h / 75 °C View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
