3-(2-甲氧基苄氧基)-1-碘丙烷合成路线 （共 5 条）
反应条件
lithium iodide in acetone
1 h; Heating;
参考文献
WARNER-LAMBERT COMPANY LLC
Patent: WO2004/89915 A1, 2004 ;
Location in patent: Page 66-67 ;
反应条件
1: 98 percent / diisobutylaluminium hydride / toluene / 18 h / 0 - 20 °C
2: 27 percent / dimethylaminopyridine; pyridine / CH2Cl2 / 24 h / Heating
3: 100 percent / lithium iodide / acetone / 1 h / Heating
View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
反应条件
1: 89 percent / benzene / 5 h / Heating
2: 98 percent / diisobutylaluminium hydride / toluene / 18 h / 0 - 20 °C
3: 27 percent / dimethylaminopyridine; pyridine / CH2Cl2 / 24 h / Heating
4: 100 percent / lithium iodide / acetone / 1 h / Heating
View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
反应条件
1: 27 percent / dimethylaminopyridine; pyridine / CH2Cl2 / 24 h / Heating
2: 100 percent / lithium iodide / acetone / 1 h / Heating
View Scheme
参考文献
Cody, Wayne L.; Holsworth, Daniel D.; Powell, Noel A.; Jalaie, Mehran; Zhang, Erli; Wang, Wei; Samas, Brian; Bryant, John; Ostroski, Robert; Ryan, Michael J.; Edmunds, Jeremy J.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 1 p. 59 - 68
反应条件
potassium carbonate in acetonitrile
18 h; Heating;
参考文献
WARNER-LAMBERT COMPANY LLC
Patent: WO2004/89915 A1, 2004 ;
Location in patent: Page 69-71 ;
