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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
77312-59-5
合成路线
（共 11 条）
89872-75-3
→
反应条件
77312-59-5
反应条件
silver carbonate in benzene 2 h; Heating;
参考文献
Rao, A V Rama; Deshpande, V H; Ravichandran, K; Rao, B Ramamohan
Synthetic Communications, 1983 , vol. 13, # 14 p. 1219 - 1224
32940-15-1
5-甲氧基-2-萘满酮
→
反应条件
77312-59-5
反应条件
1: 70 percent / acetic acid / ethanol; CHCl3 / 8 h / 25 °C 2: 86 percent / PTS-acid / CHCl3 / 6 h / Ambient temperature 3: 2.) aq. acetic acid / 1.) 25 deg C, 16 h, 2.) heating, 45 min View Scheme
参考文献
Deshpande, V.H.; Ravichandran, K.; Rao, B. Ramamohan
Synthetic Communications, 1984 , vol. 14, # 5 p. 477 - 482
2741-79-9
→
反应条件
77312-59-5
反应条件
1: 86 percent / PTS-acid / CHCl3 / 6 h / Ambient temperature 2: 2.) aq. acetic acid / 1.) 25 deg C, 16 h, 2.) heating, 45 min View Scheme
参考文献
Deshpande, V.H.; Ravichandran, K.; Rao, B. Ramamohan
Synthetic Communications, 1984 , vol. 14, # 5 p. 477 - 482
91299-84-2
→
反应条件
77312-59-5
反应条件
1: 100 percent / m-chloroperbenzoic acid / CH2Cl2 / 2.5 h 2: 80 percent / LiAlH4 / diethyl ether / Ambient temperature 3: 60 percent / Fetizon's reagent / benzene / 1.5 h / Heating View Scheme
参考文献
Rao, A. V. Rama; Chanda, Bhanu M.; Borate, Hanumant B.
Synthetic Communications, 1984 , vol. 14, # 3 p. 257 - 264
89872-74-2
→
反应条件
77312-59-5
反应条件
1: vanadium oxyacetylacetonate, tert. butyl hydroperoxide / benzene / 2 h 2: LiAlH4 / tetrahydrofuran / 4 h / Ambient temperature 3: 80 percent / Fetizon's reagent / benzene / 2 h / Heating View Scheme
参考文献
Rao, A V Rama; Deshpande, V H; Ravichandran, K; Rao, B Ramamohan
Synthetic Communications, 1983 , vol. 13, # 14 p. 1219 - 1224
91299-85-3
→
反应条件
77312-59-5
反应条件
1: 80 percent / LiAlH4 / diethyl ether / Ambient temperature 2: 60 percent / Fetizon's reagent / benzene / 1.5 h / Heating View Scheme
参考文献
Rao, A. V. Rama; Chanda, Bhanu M.; Borate, Hanumant B.
Synthetic Communications, 1984 , vol. 14, # 3 p. 257 - 264
89872-73-1
→
反应条件
77312-59-5
反应条件
1: NaBH4 / methanol / 4 h / Heating 2: vanadium oxyacetylacetonate, tert. butyl hydroperoxide / benzene / 2 h 3: LiAlH4 / tetrahydrofuran / 4 h / Ambient temperature 4: 80 percent / Fetizon's reagent / benzene / 2 h / Heating View Scheme
参考文献
Rao, A V Rama; Deshpande, V H; Ravichandran, K; Rao, B Ramamohan
Synthetic Communications, 1983 , vol. 13, # 14 p. 1219 - 1224
91299-83-1
→
反应条件
77312-59-5
反应条件
1: 98 percent / Zn(BH4)2 / diethyl ether / 2 h / Ambient temperature 2: 100 percent / m-chloroperbenzoic acid / CH2Cl2 / 2.5 h 3: 80 percent / LiAlH4 / diethyl ether / Ambient temperature 4: 60 percent / Fetizon's reagent / benzene / 1.5 h / Heating View Scheme
参考文献
Rao, A. V. Rama; Chanda, Bhanu M.; Borate, Hanumant B.
Synthetic Communications, 1984 , vol. 14, # 3 p. 257 - 264
89872-72-0
→
反应条件
77312-59-5
反应条件
1: 70 percent / NCS, AgNO3 / H2O; acetonitrile / 1 h / Ambient temperature 2: NaBH4 / methanol / 4 h / Heating 3: vanadium oxyacetylacetonate, tert. butyl hydroperoxide / benzene / 2 h 4: LiAlH4 / tetrahydrofuran / 4 h / Ambient temperature 5: 80 percent / Fetizon's reagent / benzene / 2 h / Heating View Scheme
参考文献
Rao, A V Rama; Deshpande, V H; Ravichandran, K; Rao, B Ramamohan
Synthetic Communications, 1983 , vol. 13, # 14 p. 1219 - 1224
917-64-6
magnesium,carbanide,iodide
→
反应条件
77312-59-5
反应条件
acetic acid 1.) 25 deg C, 16 h, 2.) heating, 45 min; Yield given. Multistep reaction;
参考文献
Deshpande, V.H.; Ravichandran, K.; Rao, B. Ramamohan
Synthetic Communications, 1984 , vol. 14, # 5 p. 477 - 482
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