773837-37-9合成路线 （共 596 条）
反应条件
vector pCDFDuet-HF and vector pET30-(S)-alcohol dehydrogenase in Escherichia coli BL21(DE3) in aq. buffer T=30°C; pH=7; 10 h; Enzymatic reaction; stereoselective reaction;
参考文献
Chen, Shao-Yun; Yang, Chen-Xi; Wu, Jian-Ping; Xu, Gang; Yang, Li-Rong
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3179 - 3190
反应条件
β-cyclodextrin-polyurethane polymercoated Fe3O4 magnetic nanoparticle in water T=90°C; 0.416667 h;
参考文献
Kiasat, Ali Reza; Nazari, Simin
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 365, p. 80 - 86
反应条件
(NH4)2CO3 in water T=20°C; 72 h; Cooling with ice;
参考文献
BOEHRINGER INGELHEIM INTERNATIONAL GmbH; Dahmann, Georg; Fiegen, Dennis; Fleck, Martin; Hoffmann, Matthias; Klicic, Jasna; East, Stephen Peter; Napier, Spencer Charles R.; Scott, John
Patent: US2013/23502 A1, 2013 ;
Location in patent: Paragraph 0266-0268 ;
反应条件
copper (I) cyanide T=20°C;
参考文献
Habibi, Davood; Heydari, Somayyeh; Nasrollahzadeh, Mahmoud
2012 , vol. 36, # 10 p. 573 - 574,2
反应条件
1: 2-chloro-acetophenone With alcohol dehydrogenase from Lactobacillus brevis; NADPH; isopropyl alcohol T=30°C; pH=7.5; 6 h; aq. bufferEnzymatic reaction; 2: sodium cyanide With halohydrin dehalogenase from Mycobacterium sp. GP1 T=30°C; pH=7.5; 18 h; aq. bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
European Journal of Organic Chemistry, , # 14 p. 2293 - 2298
反应条件
sodium metaphosphate; oxygen in neat (no solvent) byproducts: (CN)2; heating at 500°C, 1h;;
参考文献
Bulletin de la Societe Chimique de France, , p. 916 - 918
反应条件
byproducts: CO; Heating (1000°C) intimately ground mixt. of starting materials in molar ratio NaCN:BPO4:Na3PO4 = 1:1:1.; SEM anal.;
参考文献
Journal of the American Ceramic Society, , vol. 69, # 5 p. c. 95-c. 97
反应条件
byproducts: CO, P, N2; Heating (1000°C, 17 h, Ar or N2) intimately ground mixt. of starting materials in molar ratio NaCN:BPO4 between 1.24 and 1.714.; Removal of soluble compd. by washing a fraction of light-colored products with hot (80°C) H2O and then with acetone followed by drying of residues (120°C). XRD and EDX for solids, and Raman spectroscopy for solids and aliquots of aq. ext.;
参考文献
Journal of the American Ceramic Society, , vol. 69, # 5 p. c. 95-c. 97
反应条件
copper(l) iodide; 2,4-dimethyl-pyridine; methoxybenzene T=155°C; 12 h; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2009/85816 A1, 2009 ;
Location in patent: Page/Page column 31-32 ;
反应条件
1: in N,N-dimethyl-formamide T=60°C; 3 h; Inert atmosphere; 2: With chlorine in N,N-dimethyl-formamide T=60°C; 1 h; Inert atmosphere;
参考文献
Ihara Chemical Industry Co., Ltd.
Patent: EP2426114 A1, 2012 ;
Location in patent: Page/Page column 13 ;
