773837-37-9合成路线 （共 596 条）
反应条件
in N,N-dimethyl-formamide T=20°C; 0.5 h;
参考文献
GRUeNENTHAL GMBH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; SCHIENE, Klaus; DE VRY, Jean; DAMANN, Nils; FRORMANN, Sven; LESCH, Bernhard; LEE, Jeewoo; KIM, Yong-Soo; KIM, Myeong-Seop
Patent: WO2010/127855 A1, 2010 ;
Location in patent: Page/Page column 127; 128 ;
反应条件
tetrabutylammomium bromide in water; toluene T=55°C;
参考文献
Pan, Xianhua; Huang, Rui; Zhang, Jianshui; Ding, Liping; Li, Weijin; Zhang, Qunhui; Liu, Feng
Tetrahedron Letters, 2012 , vol. 53, # 40 p. 5364 - 5366
反应条件
in water T=-5 - 5°C; 0.666667 h;
参考文献
Okamoto, Osamu; Falgueyret, Jean-Pierre; Oballa, Renata Marcella; Prasit, Petpiboon; Rydzewski, Robert
Patent: US2003/229226 A1, 2003 ;
Location in patent: Page 8 ;
反应条件
in water byproducts: dicyan, NaBr; max.temp.20.deegree.C;
参考文献
Schulek, E.; Molnar, L.- G.
Magyar Kemikusok Lapja, 1949 , vol. 4, p. 35
C.A., 1959 , p. 969
Full Text Show Details
Gmelin Handbook: C: MVol.D3, 6.2.5.1.1, page 217 - 218
反应条件
sodium chlorate; sulfuric acid in not given
参考文献
Grignard, V.; Crouzier, P.
Bull. Soc. Chim. France (4), 1921 , vol. 29, p. 214 - 217
Full Text Show Details
Gmelin Handbook: C: MVol.D3, 6.2.5.1.2, page 218 - 219
反应条件
chlorine in water byproducts: NaCl, HCl; HBr-HCN molar ratio:1-1;
参考文献
Zmaczynski, E.
Ber. Dtsch. Chem. Ges., 1926 , vol. 59, p. 710 - 711
Full Text Show Details
Gmelin Handbook: C: MVol.D3, 6.2.5.1.2, page 218 - 219
参考文献
Mahler, E.; Dodonow, J.
Ber. Dtsch. Chem. Ges., 1926 , vol. 59, p. 2208 - 2209
Full Text Show Details
Gmelin Handbook: C: MVol.D3, 6.2.5.1.3, page 219 - 219
反应条件
in dimethyl sulfoxide T=90°C; 1 h;
参考文献
NOVARTIS AG; Bock, Mark Gary; Gaul, Christoph; Gummadi, Venkateshwar Rao; Moebitz, Henrik; Sengupta, Saumitra
Patent: US2014/45872 A1, 2014 ;
Location in patent: Paragraph 0847 ;
反应条件
in methanol T=70°C; 2 h;
参考文献
NOVARTIS AG; COPPOLA, Gary Mark; IWAKI, Yuki; KARKI, Rajeshri Ganesh; KAWANAMI, Toshio; KSANDER, Gary Michael; MOGI, Muneto; SUN, Robert
Patent: WO2010/136474 A2, 2010 ;
Location in patent: Page/Page column 180-181 ;
反应条件
chlorine in water continuous method, 15percent NaCN soln.;
参考文献
Gmelin Handbook: C: MVol.D3, 6.2.4.1.3, page 187 - 188
Full Text Show Details
Nilok Chemicals Inc.
Patent: GB967458 , 1964 ;
C.A., 1964 , vol. 61, p. 12983
