773837-37-9合成路线 （共 596 条）
反应条件
in dimethyl sulfoxide T=100°C;
参考文献
Kyowa Hakko Kirin Co., Ltd.
Patent: EP2163554 A1, 2010 ;
Location in patent: Page/Page column 56 ;
反应条件
ruthenium trichloride; oxygen; acetic acid in methanol T=60°C; P=760.051 Torr; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 130, # 33 p. 11005 - 11012
反应条件
in N,N-dimethyl-formamide T=120°C; 24 h; Inert atmosphere;
参考文献
Journal of Natural Medicines, , vol. 64, # 3 p. 245 - 251
反应条件
in methanol; water 10 h; RefluxInert atmosphere;
参考文献
Brandt, Gary E. L.; Blagg, Brian S. J.
ACS Medicinal Chemistry Letters, 2011 , vol. 2, # 10 p. 735 - 740
反应条件
tri-tert-butyl phosphine; Pd2(dba)5; zinc in tetrahydrofuran; acetonitrile T=70°C; 2 h;
参考文献
Ushkov, Alexander V.; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 28 p. 10999 - 11005
反应条件
air in neat (no solvent) heating in air at 560°C. 8h;; monitoring by IR;;
参考文献
Saita, Y.
C. A., Nagoyashi Kogyo Kenkyusho Kenkyu Hokoku Nr. 15 (1956) 26/9 1957 , p. 5672
反应条件
air in solid at temp. 390 - 570 ° C in static air atm. at heating rate 5 °/min (TG/DSC expt.);; detected by IR;;
参考文献
De Marco, D.; Marchese, A.; Migliardo, P.; Bellomo, A.
Journal of Thermal Analysis, 1987 , vol. 32, p. 927 - 938
反应条件
in ethanol react. of educts under addn. of CO, HCN or(CN)2 at 50°C; react. favoured by addn. of C, CaCO3 or MgO;;
参考文献
Gmelin Handbook: Na: SVol.4, 7, page 1382 - 1384
Full Text Show Details
N. V. Stikstofbindingsindustrie Nederland
Patent: US1971009 , 1934 ;
C. A., 1934 , p. 6254
Full Text Show Details
N. V. Stikstofbindingsindustrie Nederland
Patent: DE648497 , 1937 ;
C. II, 1937 , p. 2751
Full Text Show Details
N. V. Stikstofbindingsindustrie Nederland
Patent: FR731167 , 1932 ;
C. II, 1932 , p. 3159
Full Text Show Details
Rusting, N.
Patent: NL29812 , 1933 ;
C. II, 1933 , p. 1429
反应条件
in ethanol react. of educts under addn. of CO, HCN or(CN)2 at 50°C; react. favoured by addn. of C, CaCO3 or MgO;;
参考文献
Gmelin Handbook: Na: SVol.4, 7, page 1382 - 1384
Full Text Show Details
N. V. Stikstofbindingsindustrie Nederland
Patent: US1971009 , 1934 ;
C. A., 1934 , p. 6254
Full Text Show Details
N. V. Stikstofbindingsindustrie Nederland
Patent: DE648497 , 1937 ;
C. II, 1937 , p. 2751
Full Text Show Details
N. V. Stikstofbindingsindustrie Nederland
Patent: FR731167 , 1932 ;
C. II, 1932 , p. 3159
Full Text Show Details
Rusting, N.
Patent: NL29812 , 1933 ;
C. II, 1933 , p. 1429
反应条件
in not given byproducts: Pb; PbO reacts with molten NaCN;; extg. with boiling 80percent alcohol;;
参考文献
Gmelin Handbook: Na: MVol., 288, page 799 - 801
