hydrogenchloride in diethyl ether
T=-78 - 20°C; 12 h;
参考文献
Clark, Timothy J.; Rodezno, Jose M.; Clendenning, Scott B.; Aouba, Stephane; Brodersen, Peter M.; Lough, Alan J.; Ruda, Harry E.; Manners, Ian
Chemistry - A European Journal, 2005 , vol. 11, # 15 p. 4526 - 4534
1.1: n-BuLi / hexane; diethyl ether / 1 h / 5 °C
1.2: hexane; diethyl ether / 5 - 20 °C
2.1: 20.9 g / HCl / diethyl ether / 12 h / -78 - 20 °C
View Scheme
参考文献
Clark, Timothy J.; Rodezno, Jose M.; Clendenning, Scott B.; Aouba, Stephane; Brodersen, Peter M.; Lough, Alan J.; Ruda, Harry E.; Manners, Ian
Chemistry - A European Journal, 2005 , vol. 11, # 15 p. 4526 - 4534
