5-氯-2-羟基-3-甲氧基苯甲醛合成路线 (共 2 条)
反应条件
iodine cloride; sodium hydrogencarbonate in dichloromethane T=0°C; 0.75 h;
参考文献
Yue, Eddy W.; Gerdes, John M.; Mathis, Chester A.
Journal of Organic Chemistry, 1991 , vol. 56, # 18 p. 5451 - 5456
反应条件
1: 1) 99percent hydrazine hydrate, 2) KOH / 1) reflux, 5 h, 2) reflux, 5 h 2: 75 percent / K2CO3 / acetone / 5 h / Heating View Scheme
参考文献
Daukshas, V. K.; Martinkus, R. S.; Kuleshyus, V. A.; Shtel'bene, V. P.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, p. 458 - 463
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 3 p. 522 - 528