lithium diisopropyl amide in tetrahydrofuran
T=0°C; 0.0166667 h; various time, various molar ratio of substrates, also in the presence of DBNO; Product distributionMechanism;
参考文献
Ashby, E. C.; Deshpande, Abhay K.; Patil, Girish S.
Journal of Organic Chemistry, 1995 , vol. 60, # 3 p. 663 - 672
lithium aluminium tetrahydride in tetrahydrofuran
T=25°C; 21 h; also with LAD in THF-d8; other time; various ratio of the title compound to LAH; Product distributionMechanism;
参考文献
Ashby, E. C.; Deshpande, Abhay K.
Journal of Organic Chemistry, 1994 , vol. 59, # 14 p. 3798 - 3805
dicyclo-hexylphosphine in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=24°C; 4 h; Further byproducts given. Title compound not separated from byproducts;
