2,4,6-三氯嘧啶-5-羰酰氯合成路线 (共 2 条)
反应条件
oxalyl dichloride; N,N-dimethyl-formamide in tetrahydrofuran
T=20°C; 2.25 h;
参考文献
ABBOTT LABORATORIES; VASUDEVAN, Anil; PENNING, Thomas; CHEN, Huanming; LIANG, Bo; WANG, Shaohui; WU, Fengchun; SHEN, Yan; LIU, Cuihua; ZOU, Zhenguang
Patent: WO2012/97478 A1, 2012 ;
Location in patent: Page/Page column 56-57 ;
反应条件
sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile in anhydrous dichloroethane
T=60 - 75°C; 100 h;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2004/18435 A1, 2004 ;
Location in patent: Page 56 ;
WO 2004/018435 A1