(3-甲基-2-氧代丁基)膦酸二乙酯合成路线 （共 9 条）
参考文献
Jones, Stephen R.; Selinsky, Barry S.; Rao, Meenakshi N.; Zhang, Xuehai; Kinney, William A.; Tham, Fook S.
Journal of Organic Chemistry, 1998 , vol. 63, # 11 p. 3786 - 3789
反应条件
in dichloromethane
Ambient temperature;
参考文献
Herzig, Christian; Gasteiger, Johann
Chemische Berichte, 1982 , vol. 115, # 2 p. 601 - 614
反应条件
1: sodium iodide / methanol / 24 h / Ambient temperature
2: Ambient temperature
View Scheme
参考文献
Ryglowski, Artur; Kafarski, Pawel
Tetrahedron, 1996 , vol. 52, # 32 p. 10685 - 10692
反应条件
1: 79 percent / Triethylamin / CH2Cl2
2: 1.) Et2NH or EtOH, 2.) 10percent aq. HCl / 1.) ether, room temp., 12 h, 2.) 24h, room temp.
View Scheme
参考文献
Altenbach, Hans-Josef; Korff, Rainer
Tetrahedron Letters, 1981 , vol. 22, # 51 p. 5175 - 5178
反应条件
(i) nBuLi, hexane, THF, (ii) Cu2I2, (iii) /BRN= 605393/, Et2O; Multistep reaction;
参考文献
Mathey,F.; Savignac,P.
Tetrahedron, 1978 , vol. 34, p. 649 - 654
反应条件
hydrogenchloride; ethanol; diethylamine
1.) ether, room temp., 12 h, 2.) 24h, room temp.; Yield given. Multistep reaction;
参考文献
Altenbach, Hans-Josef; Korff, Rainer
Tetrahedron Letters, 1981 , vol. 22, # 51 p. 5175 - 5178
参考文献
Savignac,P.; Coutrot,P.
Synthesis, 1978 , p. 682 - 684
反应条件
Ambient temperature; Yield given;
参考文献
Ryglowski, Artur; Kafarski, Pawel
Tetrahedron, 1996 , vol. 52, # 32 p. 10685 - 10692
反应条件
ammonium acetate; hydrogenchloride; sodium cyanoborohydride in methanol
2.5 h; Ambient temperature;
参考文献
Varlet, J. M.; Collignon, N.; Savignac, Ph.
Tetrahedron, 1981 , vol. 37, # 21 p. 3713 - 3721
