1: With benzoyl chloride; sodium hydroxide in dichloromethane; water T=5°C; Reflux; 2: With phosphorus oxytribromide in toluene Schlenk techniqueInert atmosphereReflux;

1.1: iron sulphate heptahydrate; nitrobenzene; sulfuric acid / 20 h / 100 °C / |Reflux 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C 3.1: sodium hydroxide; benzoyl chloride / dichloromethane; water / 5 °C / |Reflux 3.2: |Schlenk technique; |Inert atmosphere; |Reflux View Scheme

T=160°C;

暂无反应条件数据