1-异丁基-1H-苯并[d]咪唑-2(3h)-酮合成路线 （共 4 条）
反应条件
copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene; L-proline in dimethyl sulfoxide
T=140°C; 0.333333 h; Microwave irradiation;
参考文献
Li, Zhaoguang; Sun, Hongbin; Jiang, Hualiang; Liu, Hong
Organic Letters, 2008 , vol. 10, # 15 p. 3263 - 3266
反应条件
hydrogenchloride in water
T=60°C; 1 h;
参考文献
Vernin, Gaston; Domlog, Hicham; Siv, Chan; Metzger, Jaques; El-Shafei, Ahmed Kamal
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 85 - 89
反应条件
1: 85 percent / 50percent aq. NaOH / triethylbutylammonium chloride / benzene / 1 h / 60 °C
2: 95 percent / conc. hydrochloric acid / H2O / 1 h / 60 °C
View Scheme
参考文献
Vernin, Gaston; Domlog, Hicham; Siv, Chan; Metzger, Jaques; El-Shafei, Ahmed Kamal
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 85 - 89
反应条件
1: 75 percent / 0.08 h / 150 °C
2: 85 percent / 50percent aq. NaOH / triethylbutylammonium chloride / benzene / 1 h / 60 °C
3: 95 percent / conc. hydrochloric acid / H2O / 1 h / 60 °C
View Scheme
参考文献
Vernin, Gaston; Domlog, Hicham; Siv, Chan; Metzger, Jaques; El-Shafei, Ahmed Kamal
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 85 - 89
