N-(2-(4-乙基-1-哌嗪基)-1-甲基乙基)-N-苯基-丙酰胺草酸盐(1:2)合成路线 (共 5 条)
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3315 - 3322
反应条件
1: 12 g / diethyl ether / 1 h / 5 °C
2: 56.4 percent / K2CO3 / ethanol / 8 h / Heating
3: 41.9 percent / LiAlH4 / tetrahydrofuran / 7 h / Heating
4: 97.8 percent / 3 h / 100 °C
5: 92.1 percent / diethyl ether
View Scheme
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3315 - 3322
反应条件
1: 56.4 percent / K2CO3 / ethanol / 8 h / Heating
2: 41.9 percent / LiAlH4 / tetrahydrofuran / 7 h / Heating
3: 97.8 percent / 3 h / 100 °C
4: 92.1 percent / diethyl ether
View Scheme
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3315 - 3322
反应条件
1: 41.9 percent / LiAlH4 / tetrahydrofuran / 7 h / Heating
2: 97.8 percent / 3 h / 100 °C
3: 92.1 percent / diethyl ether
View Scheme
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3315 - 3322
反应条件
1: 97.8 percent / 3 h / 100 °C
2: 92.1 percent / diethyl ether
View Scheme
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3315 - 3322