Zabolotskaya, N. N.; Luk'yanova, E. I.; Shoikhet, D. N.
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1943 , vol. 16, p. 118 - 128
C. A., 1944 , p. 1328
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Gmelin Handbook: Na: SVol.4, 14, page 1398 - 1400
Crespi, M.; Moles, E.
Anales Soc. Espan. Fis. Quim. (Madrid), 1922 , vol. 20, p. 555 - 562
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Gmelin Handbook: Mn: MVol.C2, 2.11.1.5.2.1.3, page 143 - 146
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反应条件
in dichloromethane
参考文献
The Research Foundation of State University of New York
Patent: US6100411 A1, 2000 ;
→
反应条件
perchloric acid; sodium perchlorate in perchloric acid dissolution of uranium oxide in hot perchloric acid, prepn. of 0.05 M aq. soln. of Na2SO4 containing 4.2 μM U(VI), prepn. of 0.1 M aq. soln. of NaClO4 containing 4.2 μM U(VI), addn. of Na2SO4 soln. to NaClO4 soln. at 10-75°C at pH 2.7-3.2; fluorescence spectroscopy;
sodium perchlorate in perchloric acid Kinetics; reaction to determine decay constants of uranyl luminescence in presence of a quencher;
参考文献
Park, Yoon-Yul; Sakai, Yoichi; Abe, Ryuji; Ishii, Takashi; Harada, Masayuki; et al.
Journal of the Chemical Society, Faraday Transactions, 1990 , vol. 86, # 1 p. 55 - 60
water in not given byproducts: Ca(OH)2; at 25 to 35°C; double salts of alkali sulfates and Ca-sulfates are also used;; ppt. is filtered, washed first with ether-ethanol mixture, then with pure ether and dried above H2SO4 in vac.;;
