sodium hydroxide in water storing a concd. soln. of Na2SO3 contg. a small amt. of NaOH in an atmosphere of NO for 5 days; starting with a overpressure of NO then storing at ambient pressure; pptn. of the sulfate on cooling at 0 °C; evapn. of the filtrate in vacuum;; formation of a crystalline crust on evaporating;;
Gmelin Handbook: S: MVol.B3, 100.101, page 1293 - 1530
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S: MVol.B3 (1963) pp. 1379-1386
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S: MVol.B3 (1963) pp. 1402-1411
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S: MVol.B3 (1963) pp. 1438-1439
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S: MVol.B3 (1963) pp. 1465-1467
catalyst: steel in not given Kinetics; byproducts: FeS; 276-316°C in steel bomb at pH=9.5-11;
参考文献
Taff, W. O.; Johnstone, H. E.; Straub, F. G.
Transactions of the ASME, 1938 , vol. 60, p. 261 - 265
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Gmelin Handbook: S: MVol.B2, 1.5.2, page 482 - 497
