in tetrahydrofuran
T=-70°C; 0.0833333 h; further solvent; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takagi, Masato; NOjima, Masamoto; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4676 - 4684
caesium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in water
T=90°C; Suzuki-Miyaura cross-coupling; 24 h; Title compound not separated from byproducts;
参考文献
Molander, Gary A.; Elia, Maxwell D.
Journal of Organic Chemistry, 2006 , vol. 71, # 24 p. 9198 - 9202
in tetrahydrofuran
T=-70°C; 0.0833333 h; further solvent; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takagi, Masato; NOjima, Masamoto; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4676 - 4684
in tetrahydrofuran
T=-70°C; 0.0833333 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takagi, Masato; NOjima, Masamoto; Kusabayashi, Shigekazu
Journal of the American Chemical Society, 1983 , vol. 105, # 14 p. 4676 - 4684
in acetonitrile
Ar atmosphere, room temp.; stirring of Cu-compd. in MeCN (10 min), addn. of soln. of org. compd. in MeCN, stirring (1 h); removal of MeCN (vac.), extn. of org. compds.;
参考文献
Jacobson, Richard R.; Tyeklar, Zoltan; Karlin, Kennth D.
Inorganica Chimica Acta, 1991 , vol. 181, p. 111 - 118